Indira Gandhi National Tribal University, Amarkantak

Prof. Ram Dayal Munda Central Library

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Sustainable Flow Chemistry: Methods and Applications.

By: Material type: TextTextPublisher: [Place of publication not identified] : John Wiley and Sons, Inc. : Wiley-VCH, 2016Description: 1 online resourceContent type:
  • text
Media type:
  • computer
Carrier type:
  • online resource
ISBN:
  • 9783527689101
  • 3527689109
Genre/Form: DDC classification:
  • 540
Online resources:
Contents:
Title Page; Copyright; Table of Contents; List of Contributors; Foreword; Background; The Book; The Chapters; Chapter 1: Flow Photochemistry -- a Green Technology with a Bright Future; 1.1 Introduction to Synthetic Organic Photochemistry; 1.2 Conventional Batch Photochemistry; 1.3 Continuous-Flow Chemistry; 1.4 Selected Examples of Photochemical Reactions under Flow Conditions; 1.5 Summary, Conclusion, and Outlook; Acknowledgments; References; Chapter 2: Continuous Flow Synthesis Using Recyclable Reaction Media; 2.1 Introduction; 2.2 Continuous Flow Reactions Using an Ionic Liquid
2.3 Continuous Flow Reactions Using a Fluorous Solvent2.4 Conclusions; References; Chapter 3: Synthesis and Application of H2O2 in Flow Reactors; 3.1 Introduction; 3.2 The Synthesis of Hydrogen Peroxide from Hydrogen and Oxygen in Flow Process with Microtechnology; 3.3 Application of Hydrogen Peroxide in Microreactors; 3.4 Conclusions; Acknowledgments; References; Chapter 4: Scale-Up of Flow Processes in the Pharmaceutical Industry; 4.1 Introduction; 4.2 Stages of Pharmaceutical Development; 4.3 Sustainability of Supply -- The Role of Continuous Processing
4.4 Comparison of Batch to Continuous Large-Scale Processing4.5 Scale-Up of a Flow Process; 4.6 Flow Processes in the Manufacture of Pharmaceuticals: Examples of Scale-Up; 4.7 Summary and Outlook on Future Scale-Up; References; Chapter 5: Organic Synthesis in Flow: Toward Higher Levels of Sustainability; 5.1 Introduction; 5.2 Semi-automated Optimization; 5.3 Self-Optimizing Microreactor Systems; 5.4 Sustainability in Microreactor Technology; 5.5 Conclusion; References; Chapter 6: Sustainable Flow Chemistry in Drug Discovery; 6.1 Introduction; 6.2 Laboratory Equipment
6.3 Advantages of Improved Sustainability6.4 Sustainable Drug Discovery; 6.5 Conclusions and Outlook; References; Chapter 7: Flow Tools to Define Waste/Time/Energy-Minimized Protocols; 7.1 Introduction; 7.2 Minimization of Solvents and Reuse of Catalytic Systems; 7.3 Time/Cost/Energy Saving Examples Using Flow Approach; 7.4 Conclusions; Acknowledgments; References; Chapter 8: The Application of Flow Chemistry in the Use of Highly Reactive Intermediates and Reagents; 8.1 Introduction; 8.2 Hydrogenation Reactions in Flow; 8.3 Carbonylation in Flow; 8.4 Organometallic Reagents in Flow
8.5 Synthesis of Azides and Diazoacetates in Flow8.6 The Use of Flow Reactors to Prepare Unstable Intermediates Using Photochemistry; 8.7 The Use of Flow Reactors to Prepare Unstable Intermediates Using Electrochemistry; 8.8 Fluorination and Trifluoromethylation in Flow; 8.9 Conclusions; Acknowledgments; References; Chapter 9: Nonconventional Techniques in Sustainable Flow Chemistry; 9.1 Introduction; 9.2 Microwave-Assisted Flow Chemistry; 9.3 Inductive Heating in Flow Chemistry; 9.4 Sonochemistry in Flow Chemistry; 9.5 Organic Electrochemistry in Flow Chemistry; 9.6 Conclusions; References
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Title Page; Copyright; Table of Contents; List of Contributors; Foreword; Background; The Book; The Chapters; Chapter 1: Flow Photochemistry -- a Green Technology with a Bright Future; 1.1 Introduction to Synthetic Organic Photochemistry; 1.2 Conventional Batch Photochemistry; 1.3 Continuous-Flow Chemistry; 1.4 Selected Examples of Photochemical Reactions under Flow Conditions; 1.5 Summary, Conclusion, and Outlook; Acknowledgments; References; Chapter 2: Continuous Flow Synthesis Using Recyclable Reaction Media; 2.1 Introduction; 2.2 Continuous Flow Reactions Using an Ionic Liquid

2.3 Continuous Flow Reactions Using a Fluorous Solvent2.4 Conclusions; References; Chapter 3: Synthesis and Application of H2O2 in Flow Reactors; 3.1 Introduction; 3.2 The Synthesis of Hydrogen Peroxide from Hydrogen and Oxygen in Flow Process with Microtechnology; 3.3 Application of Hydrogen Peroxide in Microreactors; 3.4 Conclusions; Acknowledgments; References; Chapter 4: Scale-Up of Flow Processes in the Pharmaceutical Industry; 4.1 Introduction; 4.2 Stages of Pharmaceutical Development; 4.3 Sustainability of Supply -- The Role of Continuous Processing

4.4 Comparison of Batch to Continuous Large-Scale Processing4.5 Scale-Up of a Flow Process; 4.6 Flow Processes in the Manufacture of Pharmaceuticals: Examples of Scale-Up; 4.7 Summary and Outlook on Future Scale-Up; References; Chapter 5: Organic Synthesis in Flow: Toward Higher Levels of Sustainability; 5.1 Introduction; 5.2 Semi-automated Optimization; 5.3 Self-Optimizing Microreactor Systems; 5.4 Sustainability in Microreactor Technology; 5.5 Conclusion; References; Chapter 6: Sustainable Flow Chemistry in Drug Discovery; 6.1 Introduction; 6.2 Laboratory Equipment

6.3 Advantages of Improved Sustainability6.4 Sustainable Drug Discovery; 6.5 Conclusions and Outlook; References; Chapter 7: Flow Tools to Define Waste/Time/Energy-Minimized Protocols; 7.1 Introduction; 7.2 Minimization of Solvents and Reuse of Catalytic Systems; 7.3 Time/Cost/Energy Saving Examples Using Flow Approach; 7.4 Conclusions; Acknowledgments; References; Chapter 8: The Application of Flow Chemistry in the Use of Highly Reactive Intermediates and Reagents; 8.1 Introduction; 8.2 Hydrogenation Reactions in Flow; 8.3 Carbonylation in Flow; 8.4 Organometallic Reagents in Flow

8.5 Synthesis of Azides and Diazoacetates in Flow8.6 The Use of Flow Reactors to Prepare Unstable Intermediates Using Photochemistry; 8.7 The Use of Flow Reactors to Prepare Unstable Intermediates Using Electrochemistry; 8.8 Fluorination and Trifluoromethylation in Flow; 8.9 Conclusions; Acknowledgments; References; Chapter 9: Nonconventional Techniques in Sustainable Flow Chemistry; 9.1 Introduction; 9.2 Microwave-Assisted Flow Chemistry; 9.3 Inductive Heating in Flow Chemistry; 9.4 Sonochemistry in Flow Chemistry; 9.5 Organic Electrochemistry in Flow Chemistry; 9.6 Conclusions; References

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